Ungahlola kanjani okuqukethwe komlotha we-Hydroxypropyl Methylcellulose (HPMC)?

Ukuhlola okuqukethwe komlotha we-Hydroxypropyl Methylcellulose (HPMC) kuhlanganisa ukunquma iphesenti lensalela ye-inorganic esele ngemuva kokuba izingxenye ze-organic sezishisiwe. Nansi inqubo evamile yokuhlola okuqukethwe komlotha kwe-HPMC:

Izinto Ezidingekayo:

1. Isampula ye-Hydroxypropyl Methylcellulose (HPMC).
2. Isithando se-muffle noma isithando somlilo
3. I-crucible nesivalo (eyenziwe ngezinto ezingasebenzi njenge-porcelain noma i-quartz)
4. I-Desiccator
5. Ibhalansi yokuhlaziya
6. Isikebhe esivuthayo (uma uthanda)
7. Izibambi noma izibambi

Inqubo:

1. Ukukalwa kwesampula:
   • Kala i-crucible engenalutho (m1) uye ku-0.1 mg eseduze usebenzisa ibhalansi yokuhlaziya.
   • Beka inani elaziwayo lesampula le-HPMC (ngokuvamile amagremu angu-1-5) ku-crucible futhi urekhode isisindo esihlanganisiwe sesampula ne-crucible (m2).
2. Inqubo ye-ashing:
   • Beka i-crucible equkethe isampula ye-HPMC esithandweni somlilo noma esithandweni somlilo.
   • Shisisa isithando somlilo kancane kancane ekushiseni okucacisiwe (imvamisa engu-500-600 ° C) futhi ugcine lokhu kushisa isikhathi esinqunyiwe (ngokuvamile amahora angu-2-4).
   • Qinisekisa ukushiswa okuphelele kwezinto eziphilayo, ushiye umlotha wezinto ezingaphili kuphela.
3. Ukupholisa nokukala:
   • Ngemuva kokuthi inqubo yokuqothula isiphelile, susa i-crucible esithandweni usebenzisa ama-tongs noma abanikazi be-crucible.
   • Beka i-crucible nokuqukethwe kwayo ku-desiccator ukuze kuphole ekamelweni lokushisa.
   • Uma usupholile, kala kabusha insalela ye-crucible kanye nomlotha (m3).
4. Ukubala:
   • Bala okuqukethwe komlotha wesampula ye-HPMC usebenzisa ifomula elandelayo: Okuqukethwe komlotha (%) = [(m3 - m1) / (m2 - m1)] * 100
5. Ukutolika:
   • Umphumela otholiwe umele iphesenti lokuqukethwe komlotha wezinto ezingaphili okhona kusampula ye-HPMC ngemva kokusha. Leli nani likhombisa ubumsulwa be-HPMC kanye nenani lensalela yezinto ezingaphili ezikhona.
6. Ukubika:
   • Bika inani lokuqukethwe komlotha kanye nanoma yimiphi imininingwane efanele njengezimo zokuhlola, ukuhlonza isampula, nendlela esetshenzisiwe.

Amanothi:

• Qinisekisa ukuthi i-crucible nesivalo kuhlanzekile futhi akungcoliswanga ngaphambi kokusetshenziswa.
• Sebenzisa isithando somlilo se-muffle noma isithando somlilo esinamandla okulawula izinga lokushisa ukuze uqinisekise ukushisa okufanayo kanye nemiphumela enembile.
• Phatha i-crucible nokuqukethwe kwayo ngokucophelela ukuze ugweme ukulahleka kwezinto noma ukungcoliswa.
• Yenza inqubo yomlotha endaweni enomoya omuhle ukuze uvimbele ukuchayeka emikhiqizweni evuthayo.

Ngokulandela le nqubo, ungakwazi ukunquma ngokunembile okuqukethwe komlotha wamasampula e-Hydroxypropyl Methylcellulose (HPMC) futhi uhlole ubumsulwa nekhwalithi yawo.